Organic Structure Determination Using 2-D NMR Spectroscopy: A Problem-Based Approach - Softcover

Simpson, Jeffrey H.

Softcover

ISBN 10: 0123849705 ISBN 13: 9780123849700

Verlag: Academic Press, 2011

Inhaltsangabe

Organic Structure Determination Using 2-D NMR Spectroscopy: A Problem-Based Approach, Second Edition, provides an introduction to the use of two-dimensional (2-D) nuclear magnetic resonance (NMR) spectroscopy to determine organic structure. The book begins with a discussion of the NMR technique, while subsequent chapters cover instrumental considerations; data collection, processing, and plotting; chemical shifts; symmetry and topicity; through-bond effects; and through-space effects. The book also covers molecular dynamics; strategies for assigning resonances to atoms within a molecule; strategies for elucidating unknown molecular structures; simple and complex assignment problems; and simple and complex unknown problems. Each chapter includes problems that will enable readers to test their understanding of the material discussed.

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Über die Autorin bzw. den Autor

Jeffrey H Simpson, PhD, was Director of the Instrumentation Facility in the Department of Chemistry at M.I.T. from 2006 to 2017. Dr. Simpson’s career in NMR/instrumentation research and instruction spans 20 years, and he has authored an introductory text on the subject of NMR as well as publishing a number of peer-reviewed articles. He is one of the Founding Members of the New England NMR Society and served as VP from its inception to 2017. He currently is a faculty member in the Department of Chemistry at the University of Richmond.

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Ideal for advanced undergraduate and graduate courses in organic spectroscopy, this book provides the analytical skills and methodologies needed to assign nuclear magnetic resonances to known and unknown molecular structures. Part I covers the essential knowledge along with worked examples synthetic organic chemists should possess to understand and apply NMR in their research. Part II presents a comprehensive selection of 40 problems (20 knowns and 20 unknowns), consisting of 1H and 13C 1-D spectra plus multiple 2-D spectra.

While most books on the subject focus on mathematically rigorous treatments, this text balances rigor with guidance, providing novice and experienced chemists with the tools needed to understand and interpret 2-D NMR spectra.
? Optimizes workflow by presenting strategies for assigning resonances to known structures and for deducing structures of unknown organic molecules based on their NMR spectra
? Improves analytical and interpretation skills through the use of extensive examples and problem-solving techniques
? Enhances understanding through detailed explanations of key concepts, including an extensive glossary

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Details zur Ausgabe

• Verlag: Academic Press
• Erscheinungsdatum: 2011
• ISBN 10: 0123849705
• ISBN 13: 9780123849700
• Einband: Tapa blanda
• Sprache: Englisch
• Auflage: 2
• Anzahl der Seiten: 590
• Kontakt zum Hersteller: Nicht verfügbar