Modification of an Nbs Reference Spectrophotometer (Classic Reprint) - Softcover

Eckerle, Kenneth L.

 
9781390476293: Modification of an Nbs Reference Spectrophotometer (Classic Reprint)

Inhaltsangabe

Excerpt from Modification of an Nbs Reference Spectrophotometer<br/><br/>A pneumatically controlled sliding sample holder was constructed. The temperature of samples mounted in this holder is controlled by water circulated in the holder and in a jacket surrounding the filter to also maintain the temperature of the air surrounding the filter. The holder  jacket combination is three point spring loaded. The circulating water temperature is provided by a bath which was modified. The heaters and refrigerator (approximately 670 watts each) of the bath were isolated and ad justed so that in combination they yield a nearly constant temperature. Then, a 300 watt heater was installed to tune the temperature to the desired level. A special proportional controller was obtained which shuts off the heater or refrigerator (depending on whether one desires a lower or higher temperature) for large temperature changes (several degrees C) until the temperature reaches the range where the 300 watt heater is cycled to maintain a constant temperature as detected by a thermistor placed in the bath.

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