Nuclear magnetic resonance spectroscopy is one of the most important analytical methods available today. This practice-oriented textbook aims at teaching the use of NMR spectra in the elucidation of organic structures. The emphasis of NMR – from Spectra to Structures is on practical rather than on theoretical aspects, which are treated only briefly. The book is intended as a practical guide to today’s standard NMR experiments for students and laboratory personnel. A set of thirty-five graded problems reinforces the reader’s understanding of how problems of structure elucidation are solved by using NMR.
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Introduction
Part I - NMR Experiments
1. 1D Experiments
2. 2D Experiments
3. Quadrupolar Nucleus Experiments
4. HPLC-NMR Coupling
Appendix: Reference List
Part II - Worked Example and Problems
Introduction
Worked Example
Problems
Index
NMR spectroscopy is one of the most important analytical methods available today. This practise-oriented textbook aims at teaching the use of NMR spectra in the elucidation of organic structures.
The emphasis of the book is on practical rather than on theoretical aspects, which are treated only briefly, and it is intended as a practical guide to today’s standard NMR experiments for students and laboratory personnel.
The set of 35 graded problems includes not only the 1D NMR spectra (proton, carbon, DEPT/APT) but, for the first time in a textbook, also the most important 2D spectra (H,H and C,H correlation).
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